Thermoluminescence (TL) and Optically Stimulated Luminescence (OSL) Dating

Thermoluminescence (TL) and
Optically Stimulated Luminescence (OSL)

Luminescence dating, including thermoluminescence (TL) and optically stimulated luminescence (OSL), allows for the dating of materials that have been heated or exposed to natural light.

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Scientific equipment for thermoluminescence measurement used in material and archaeological dating

The principles of luminescence dating

Luminescence dating is a dating method based on measuring the energy accumulated in quartz or feldspar crystals present in certain materials. This energy comes from natural exposure to environmental radioactivity and is released upon exposure to heat (TL) or light (OSL). It allows us to determine the last "zeroing event" experienced by the material:

  • For thermoluminescence (TL): this refers to the last firing or heating (hearth, oven, fire),
  • For the OSL: from the last exposure to daylight (sedimentary deposit).

This method allows materials to be dated over periods of up to 700,000 years, depending on the type of sediment and preservation conditions. CIRAM rigorously adapts its protocols according to the context (museum or excavation), the type of object, and the method chosen (TL test, TL dating, or OSL).

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Thermoluminescence dating: state-of-the-art analysis

The quality of a thermoluminescence TL or OSL datingrests on three pillars:

  1. Rigorous sampling, carried out according to scientific protocols to preserve sample integrity;
  2. Highly specialized instrumentation, notably the LexsygSmart system, for precise and reliable analyses;
  3. A methodology in line with public laboratory standards, guaranteeing results that can be used for research or heritage appraisal.

CIRAMis today the only private laboratory in Europe to offer TL/OSL datingcomparable to the protocols of public research centers.

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What are the differences between TL dating and TL testing?

01 - Measuring the archaeological dose

The archaeological dose, or equivalent dose, corresponds to the energy accumulated since the last heating or insolation. This measurement is carried out in our laboratories using the LexsygSmart system, after rigorous sample treatment.

  • Test TL: the sample is subjected to a standard chemical treatment. Only 4 aliquots (sub-samples) are analyzed. The test provides an age index to detect modern objects.
  • TL dating: a precise granulometric sorting (40–120 µm) is performed and at least 40 aliquots are measured. This approach allows for reliable absolute dating.

02 - Annual radiation dose

To obtain absolute dating, it is necessary to know not only the equivalent dose but also the annual dose rate received by the object. This dose comes from three sources: the object itself (auto-irradiation), its environment (up to 1 meter), and cosmic radiation.

  • In a TL/OSL dating ..., our scientists analyze the concentration of radioelements (uranium, thorium, potassium) in the object and its environment, in order to calculate precisely this annual dose.
  • In a TL test, this value is estimated (often between 3 and 5 mGy/year), which gives an approximation of age, but not an absolute dating.

03 - X-rays, CT scans and carbon-14 to complement thermoluminescence

CIRAM combines complementary methods with TL/OSL dating, depending on the case:

  • In art, X-ray radiography and CT scanning (CT) reveal restorations, internal structures, and manufacturing processes of terracotta, ceramic, or porcelain objects.
  • In archaeology, a cross-analysis with carbon 14 can be performed on the organic materials present, allowing for a more complete and reliable dating of the context studied.

CIRAM, a reference in TL/OSL luminescence dating

Thanks to its scientific expertise and rigorous protocols, CIRAM stands out as a benchmark in radiocarbon dating, but also in luminescence dating. And for good reason, CIRAM is one of the few private laboratories to offer a complete range of TL and OSL dating services, with protocols as rigorous as those used in public laboratories.

Our expertise lies in two main areas:

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Are you asking yourself these questions?

What's the difference between a TL test and TL dating?

The TL test is a preliminary examination to assess whether a sample is old or not. TL dating, on the other hand, involves in-depth analysis with a rigorous protocol, including the precise calculation of archaeological dose and annual dose to provide a reliable absolute age.

How accurate is thermoluminescence dating?

Accuracy depends on the context and condition of the sample. In general, it varies between 5 and 10% of the estimated age.

What objects can be dated using thermoluminescence?

TL is used to date heated ceramics, terracotta, porcelain and minerals. OSL is used for sediments and minerals exposed to light.

How long does it take to obtain the results of a TL/OSL test and dating?

A TL test takes a maximum of 2 weeks, whereas TL or OSL dating takes 4 to 6 months. Turnaround times may vary according to the type of sample, the complexity of the analysis and the volume of requests.

How much does TL/OSL dating cost?

The cost of TL/OSL dating depends on the nature of the sample, the complexity of the analysis and the number of samples to be analyzed. Please contact us for a personalized quotation.

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