Archaeological mortar sample used for radiocarbon dating and chronological analysis of historic buildings

Analyzing old mortars

At CIRAM, we put materials science at the service of archaeologists, heritage architects, and historians to date ancient constructions through mortar analysis.

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They trust us

Museums, DRACs, architects of historic monuments, local authorities and research institutes call on CIRAM for the scientific study of ancient materials.

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Ancient mortar fragment from an archaeological site

Do you want to analyze old mortars?

The mortars used in ancient constructions preserve valuable information about the period when a building was constructed. By analyzing their composition and measuring their age, it is possible to:

  • Date the construction or restoration phases of a building,
  • Detect subsequent additions or modifications,
  • Understand traditional manufacturing techniques.

At CIRAM, we help heritage professionals, architects and cultural and cultural institutions in the physico-chemical analysis and dating of mortars, using a rigorous, documented scientific approach.

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Microscopes used during an experiment

Our analysis techniques for studying old mortars

CIRAM implements several complementary methods to analyze ancient mortars:

  • Composition analysis: identification of binders (lime, plaster, old cement), aggregates (sand, crushed stone), additives, pigments.
  • Radiocarbon dating of mortar: measurement of carbon 14 present in the carbonate fraction of the lime binder (formed during setting) or in charcoal.
  • Microscopy and petrography: study of internal structures, inclusions and porosity.
  • SpectroscopyandX-ray diffraction: identification of mineral phases.

These analyses make it possible to date the mortars, distinguish original materials from later interventions, and better understand ancient know-how.

Find out more about our analysis of old materials

The steps in a CIRAM analysis

Our analytical approach is based on a proven protocol:

01 - Definition of objectives

We clarify your requirements (dating, composition) and select the most appropriate method.

02 - Sampling

We will tell you precisely how to collect the mortar fragments, or we will intervene on-site if necessary.

03 - Laboratory preparation

Separation of fine fractions, removal of contaminants, particle size sorting.

04 - Analysis

Implementation of chosen techniques (carbon 14, chemical analysis, microscopy...).

05 - Scientific report

Dating, analysis, interpretation, recommendations and visual support.

Why choose CIRAM for analysis of old mortars?

By choosing CIRAM, you benefit from:

  • Recognized expertise: over 20 years of experience in dating of materials archaeological .
  • A multidisciplinary approach: combining archaeometry, chemistry, geology, and heritage.
  • Specialized equipment: adapted to old materials and fine analysis.
  • Usable deliverables: clear results, useful for restoration files, scientific publications or heritage appraisals.
  • A team that listens: we work closely with architects, curators, researchers and clients.
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Are you asking yourself these questions?

Can you really date old mortar?

Yes, by carbon-14 dating the lime binder formed during hardening, provided the mortar has not been contaminated. Or by carbon-14 dating of charcoal in the mortar.

What types of mortar can be analyzed?

Lime, plaster or cement mortars used in masonry, rendering or stone joints.

How much should I take?

Approx. 100 grams of mortar per analysis. We advise you on how to sample cleanly and efficiently.

What is the analysis time?

Allow 3 weeks on average, depending on the methods used.

Can restoration phases be detected?

Yes, by comparing several samples and cross-referencing the results, it is possible to distinguish between work campaigns.

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